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Bunker Fuel Quality

Gard: IMO updates fuel oil sampling guidelines

‘MARPOL delivered sample’ size has increased from 400ml to 600ml and must now also be available for checking the flashpoint requirements under SOLAS Regulation II-2/4.2.1, says Gard.

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Maritime protection and indemnity (P&I) club Gard on Thursday (31 November) published an insight on changes to the International Maritime Organization’s (IMO) guidelines for fuel oil sampling:

Safety of ships relating to the use of fuel oil

The minimum 60 degrees Celsius (°C) flashpoint limit in SOLAS Regulation II-2/4.2.1.1 is not new, but the regulations designed to prevent the supply of oil fuel in breach of this limit are. 

In November 2022, the IMO MSC 106 adopted amendments to SOLAS requiring bunker suppliers to provide ships with a declaration prior to bunkering, stating that the flashpoint of the actual oil fuel batch is in conformity with the flashpoint requirements of SOLAS. 

They also clarify that the required information “may be included in the Bunker Delivery Note (BDN) according to MARPOL Annex VI/18”. These SOLAS amendments will enter into force on 1 January 2026.

Information to be included in the BDN

Even though the SOLAS amendments have yet to take effect, the new flashpoint documentation requirements for suppliers became effective on 1 May 2024 in an amendment to MARPOL Annex VI. Hence, Appendix V of MARPOL Annex VI already requires the BDN to include information about the fuel oil’s flashpoint, which can be either the flashpoint value measured in °C or a general statement confirming that flashpoint has been measured at or above 70°C. 

New sampling guidelines

To support the regulatory changes, and to account for situations in which oil fuel with a flashpoint of less than 60°C has been delivered, the IMO has published a circular, MSC-MEPC.2/Circ.18, updating its fuel oil sampling guidelines. The new circular revokes the previous MEPC Resolution 182(59), the 2009 Guidelines for the safe taking of the ‘MARPOL delivered sample’, and extend the use of this sample to include testing of the SOLAS flashpoint requirements.

While the main objectives of the new guidelines and their basic requirements on sampling locations, arrangements, and procedures for taking, labelling and storing the sample, have not changed, it is important to be aware of the following changes:

Sampling methods: Section 4 explicitly requires personnel responsible for primary sampling and preparing the samples for storage to be familiar with equipment and guidelines. Also, representatives of both the ship and supplier should witness the sampling operation.

Sampling and sampling integrity: Section 5 warns against using low-flashpoint solvents to clean samplers and containers prior to use, as this can contaminate samples. 

Retained sample handling: Section 7 requires a minimum sample size of 600ml, up from 400ml previously. 

Retained sample storage: Section 9 transfers responsibility for tracking retained samples from the ship’s Master to the Company. 

Procedures and documentation following testing of retained sample: New Section 10 describes the procedures and documentation requirements for situations requiring a fuel oil’s flashpoint to be checked. The sulphur verification procedures detailed in Appendix VI of MARPOL Annex VI remain unchanged.

Furthermore, keep in mind that the retained ‘MARPOL delivered sample’ should only be used to test for compliance with the convention requirements and not to resolve commercial quality disputes. 

 

Photo credit: william william on Unsplash
Published: 5 November, 2024

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Research

Integr8 Fuels report shares comprehensive analysis of Mediterranean ECA

Data reveals a market in rapid transition, confirming some industry predictions while uncovering new, emerging risks for ship operators.

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Integr8 Fuels trading intelligence (July 2025)

International bunker trading firm Integr8 Fuels on Monday (7 July) shared its new report ‘Mediterranean ECA: Immediate Operational and Commercial Impact of Implementation’ which provides the first comprehensive analysis of the rule’s effects on fuel quality and regional availability.

The data reveals a market in rapid transition, confirming some industry predictions while uncovering new, emerging risks for ship operators. The following key findings include:

  1. Dramatic Supply Shift Confirmed: VLSFO Availability Contracts Sharply. VLSFO’s share of the Mediterranean fuel market has plummeted from over 60% in December to just 37.5% in May. In parallel, the number of ports supplying VLSFO has fallen by 47%, creating new logistical challenges for vessels that continue to use the grade.
  2. VLSFO Instability Spikes as Supply Chain Adapts. Very Low Sulphur Fuel Oil (VLSFO) off specification rates more than doubled from 1.5% in December to 3.8% in May. Critically, one in four (25%) of these off-specs were for total sediment potential (TSP), indicating a rising risk of sludge formation that can damage engines. This trend appears linked to extended in-tank storage and the consolidation of older fuel stocks as demand slows and suppliers pivot away from VLSFO.
  3. Persistent Flash Point Risks in Key LSMGO Hubs. Flash point non-conformance has increased significantly and now accounts for over two-thirds of all LSMGO off specs. Our data shows this is not a random problem, with over 75% of all flash point incidents concentrated in Spain, Turkey, and Italy, signalling a persistent potential for SOLAS violations in core supply zones.

Note: The full report may be obtained from Integr8 Fuels here.

 

Photo credit: Integr8 Fuels
Published: 8 July 2025

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Contamination

VPS advises on effects of FAME contamination in bio bunker fuels on engine oils

Stanley George highlights that engines operating on FAME-based bio bunker fuels are more susceptible to rapid oil viscosity degradation, where FAME does not evaporate easily, leading to cumulative effects.

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VPS

Stanley George, Group Science & Technical Manager of marine fuels testing company VPS, on Monday (23 June) highlighted engines operating on FAME-based biofuels are more susceptible to rapid oil viscosity degradation, where FAME does not evaporate easily, leading to cumulative effects:

Engines running on Bio-blends containing Fatty Acid Methyl Esters (FAME), especially pure FAME, e.g. 100% FAME can experience decreased engine oil viscosity over time.

Fuel oil contamination in engine lubricants is a known phenomenon, and most marine-grade engine oils are formulated to tolerate certain levels of such contamination while maintaining operational performance.

The impact of FAME contamination is more pronounced in four-stroke trunk piston engines due to their design and operational characteristics. These engines use a common oil sump for both crankcase and cylinder lubrication, making them more vulnerable to fuel ingress through injector leaks or blow-by gases. Unlike two-stroke crosshead engines, which have separate lubrication systems that limit fuel-oil interaction, four-stroke engines continuously recirculate the same oil, allowing FAME (which has a high boiling point and low volatility), to accumulate over time. This leads to a more significant reduction in oil viscosity and faster degradation of lubricating properties.

A typical SAE (Society of Automotive Engineers) 30 grade engine oil has a viscosity of about 90 to 110 cSt at 40°C and a B100 (100% FAME) or its fossil counterpart such as DMA (distillate fuel) has a viscosity in the range of 4 cSt at 40°C. Any contamination of the fuel (distillate or Bio distillate blends contain FAME) into the used engine oil can therefore significantly reduce the viscosity of the used engine oil.

Most OEMs specify both minimum and maximum viscosity limits for engine oils, beyond which the engine must not be operated to avoid wear or lubrication failure. For example, a common condemning limit is a 25% reduction in viscosity at 40°C from the fresh oil value. In the case of an SAE 30 grade oil (with a typical fresh viscosity of around 90 cSt at 40°C), this corresponds to a minimum allowable limit of approximately 67 cSt.

When comparing the viscosities of distillate fuel and B100, there is no significant difference (both typically range between 3 to 5 cSt at 40°C). However, a noticeable drop in engine oil viscosity is not usually observed when engines operate on conventional distillate fuel. This is likely due to the higher volatility and lighter fractions present in fossil fuels, which tend to evaporate over time. Additionally, the routine top-up of fresh oil during engine operation, needed to compensate for losses from evaporation and leakage, helps maintain a more stable overall oil viscosity. As a result, the dilution effect is minimised, and the lubricating oil retains its properties for a longer duration compared to operation on B100.

Distillation Behaviour Analysis of FAME

ISO 3405 is an international standard that outlines a laboratory method for determining the distillation characteristics of petroleum and related products at atmospheric pressure. This tests helps us to understand the composition and behaviour of fuel during storage and use including the tendency to form vapours.

Typically in this method, the sample is distilled under controlled conditions. Throughout the distillation, the temperature at which specific volumes of the sample evaporate is recorded. Key measurements include, Initial Boiling Point (IBP) -Temperature at which the first drop of condensate is collected, Final Boiling Point (FBP) -Temperature at which the last drop of liquid evaporates and temperature at Specific Recovery Percentages, temperatures corresponding to 10%, 50%, and 90% volume recovery, among others. The collected data is used to construct a distillation curve, which illustrates the boiling behaviour of the sample.

In order to understand this phenomenon we compared the distillation characteristic of a 100% FAME (B100), 30% FAME (B30) and pure straight run distillate fuel using the ISO 3405 method. Below is a graph illustrating the differences in the distillation characteristics.

VPS advises on effects of FAME contamination in bio bunker fuels on engine oils

Note: The full article by VPS can be viewed here

 

Photo credit: VPS
Published: 24 June, 2025

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Methanol

Auramarine launches water in methanol measurement technology

Water Content Analyser technology measures and reports concentration of water in methanol when used as a marine fuel, helping ship operators take action to minimise associated risks and costs.

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Auramarine launches water in methanol measurement technology

Finland-based fuel supply systems provider Auramarine on Tuesday (3 June) announced the launch of its Auramarine Water Content Analyser (AM Water Content Analyser). 

The technology measures and reports the concentration of water in methanol, helping ship operators take preventive action to minimise associated risks and costs when using the fuel. 

The analyser comes in response to growing uptake of methanol as a marine fuel to meet shipping’s decarbonisation targets. Water as a natural contaminant of methanol may be present in the bunkered methanol either by accident or intentionally. Water in fuel decreases the calorific heating value which increases the bunkering costs. In addition, if the water content is too high, operators may have to unload the fuel, leading to delays and additional costs.  

As an example, when a Ro-Ro vessel consumes 27 000 metric tonnes (mt) of green methanol in one year and with an average price per ton of green methanol at EUR 1,196 (USD 1,361), the operator of the vessel may avoid losses of up to EUR 1,614,600 for 5% concentration of water as contaminant. 

The AM Water Content Analyser is an inline measurement device that can be installed directly to the methanol process piping, for example to the main bunker line with the flanged housing. The technology uses a sensor to analyse the concentration of water in the methanol.

John Bergman, CEO of Auramarine, said: “Methanol uptake is increasing across the industry due to its promising Greenhouse Gas (GHG) emissions reduction credentials. At Auramarine, we’ve led the way in developing solutions that support the use of alternative fuels-starting with the industry’s first Methanol Fuel Supply Units in 2022. 

“Now, with the launch of our AM Water Content Analyser, we’re giving ship owners and operators the tools they need to take the next step in their energy transition and bunker methanol with greater confidence, and importantly, at a lower cost.”

 

Photo credit: Auramarine
Published: 4 June, 2025

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